图3.2不同反应时间产物的XRD图
图3.2是不同反应时间产物的XRD图,从图3.2中可知在反应物与熔融盐比为1:2、反应温度为1000℃、分别在1h、2h、3h、4h、5h、8h、9h、10h所得产物中除La2Zr2O7
表3.1不同反应时间产物的数据表
hkl 标准 1h 2h 3h 4h 5h 8h 9h 10h
ZrO2(001) 17.483 17.51172 17.49500413 17.5117154 17.5117154 17.49500413 17.49500413 17.47829286 17.49500413
ZrO2(110) 24.072 24.21293 24.12937792 24.07924411 24.12937792 24.07924411 24.14608919 24.12937792 24.06253284
ZrO2(011) 24.472 24.59729 24.5137371 24.74769487 24.48031457 24.58058218 24.49702583 24.5137371 24.48031457
ZrO2(-111) 28.214 28.37404024 28.29048389 28.29048389 28.30719516 28.35732897 28.30719516 28.32390643 28.24035009
ZrO2(111) 31.492 31.61602642 31.53247007 31.56589261 31.54918134 31.58260388 31.51575881 31.58260388 31.465625
ZrO2(200) 34.197 34.28982946 34.22298438 34.23969565 34.22298438 34.27311819 34.18956184 34.22298438 34.1561393
ZrO2(020) 34.401 34.50707595 34.44023088 34.47365341 34.45694215 34.40680834 34.44023088
ZrO2(002) 35.335 35.35935067 35.39277321 35.40948448 35.40948448 35.42619575 35.35935067 35.35935067 35.3426394
ZrO2(-201) 35.922 35.91082255 35.94424508 35.92753382 35.91082255 35.94424508
ZrO2(120) 38.589 38.60133685 38.65147066 38.61804812 38.61804812 38.60133685
ZrO2(012) 39.474 39.50374538 39.4369003 39.47032284 39.45361157 39.48703411 39.45361157 39.48703411 39.48703411
ZrO2(-112) 40.765 40.90749197 40.82393563 40.75709055 40.80722436 40.8406469 40.79051309 40.79051309 40.79051309
ZrO2(201) 41.213 41.24171735 41.22500608 41.20829481 41.22500608 锆酸镧陶瓷粉的制备+文献综述(8):http://www.youerw.com/huaxue/lunwen_1876.html